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Girolami, G.S. Holmes, Stephen Michael 2015-09-25T22:14:35Z 2015-09-25T22:14:35Z 2000 2000 Improved preparations are given for several first-row transition metal trifluoromethanesulfonate (OTf) and p-toluenesulfonate (OTs) salts: M(OTf)x, where M = VII, VIII, CrII, MnII, CoII, NiII , and Cs, and [M(OH2)n][OTs]x, where M = TiIII, VIII, VIVO, Cr II, CrIII, MnII, FeII, CoII, NiII, and Cs. Also described are preparations of the cyanide building blocks K4[V(CN)6]·xH 2O, [NEt4]4[V(CN)6], K3[Cr(CN) 6]·xH2O, [NEt4]3[Cr(CN) 6]·xH2O, [NEt4]3[Ti(CN) 6]·2.5H2O, [PPN]3[Cr(CN)6], [PPN]3[Fe(CN)6], [NEt4]3[Co(CN) 6]·H2O, [PPN]3[Cr(CN)5NO], [NEt 4]CN, and [PPN]CN. Made available in DSpace on 2015-09-25T22:14:35Z (GMT). No. of bitstreams: 2 license.txt: 4848 bytes, checksum: 96035ab3f5e1c23cc7138a224ce498bd (MD5) 9953048.pdf: 10279021 bytes, checksum: 50ba3a572fe659ee2b445e7ef839c0a5 (MD5) Previous issue date: 2000 Embargo set by: Seth Robbins for item 85737 Lift date: Forever Reason: Restricted to the U of I community idenfinitely during batch ingest of legacy ETDs Open Restriction set for Item 85737 on 2020-06-17T18:57:11Z with date null by bran3@illinois.edu. Author gave express permission to lift restriction. Open 298 p. Thesis (Ph.D.)--University of Illinois at Urbana-Champaign, 2000. http://hdl.handle.net/2142/84456 (MiAaPQ)AAI9953048 eng Physics, Electricity and Magnetism Molecule-Based Magnets Constructed From Hexacyanometalates text Chemistry Chemistry University of Illinois at Urbana-Champaign Dissertation Ph.D.