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oai:www.ideals.illinois.edu:2142/84491 2023-07-11 col_2142_5131 col_2142_14789 com_2142_5130 com_2142_14788 com_2142_8903

Klemperer, Walter G. Pafford, Margaret Mary Elizabeth 2015-09-25T22:14:47Z 2015-09-25T22:14:47Z 10000-01-01 2000 2000 The ambient temperature hydrolysis product of tetra-n-propyl orthozirconate was identified as [Zr3O](OPrn) 10 by 13C NMR spectroscopy and elemental analysis. Ethanolysis of [Zr3O](OPrn) 10 yielded the ethoxy derivative of the trizirconate which was characterized by 13C NMR spectroscopy and elemental analysis. Reaction of the trizirconates with the parent alcohol resulted in the formation of alcohol adducts which are thought to have structures similar to that reported for {[Hf3O](OEt)10(EtOH)}2. Made available in DSpace on 2015-09-25T22:14:47Z (GMT). No. of bitstreams: 2 license.txt: 4848 bytes, checksum: 96035ab3f5e1c23cc7138a224ce498bd (MD5) 9990102.pdf: 3685291 bytes, checksum: 337ead1cc8eac937513613db29d4d48f (MD5) Previous issue date: 2000 Embargo set by: Seth Robbins for item 85772 Lift date: Forever Reason: Restricted to the U of I community idenfinitely during batch ingest of legacy ETDs Restricted to the U of I community idenfinitely during batch ingest of legacy ETDs U of I Only 167 p. Thesis (Ph.D.)--University of Illinois at Urbana-Champaign, 2000. http://hdl.handle.net/2142/84491 (MiAaPQ)AAI9990102 eng Chemistry, Inorganic Synthesis and Characterization of Alkyl Tetra-, Tri-, and Triskaidecazirconates text Chemistry Chemistry University of Illinois at Urbana-Champaign Dissertation Ph.D.